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Beilstein J. Org. Chem. 2019, 15, 558–566, doi:10.3762/bjoc.15.50
Graphical Abstract
Figure 1: a) CAD drawing of the reactor R1. b) 3D-printed reactor R1 from the CAD drawing. The reactor is fil...
Figure 2: a) L-shaped rail made of PLA with the mounted reactor R3. The small picture shows the fixed reactor...
Figure 3: a) Microreactor R4 with a reactor volume of 12 µL filled with a blue dye solution. b) Magnification...
Figure 4: CAD drawing of two CSTR with three (a) and two inlets (b) with in-printed screw nuts 1/4’’ – 28 thr...
Figure 5: a) Unassembled parts used for one syringe pump. b) Assembled pump with controller.
Scheme 1: Preparation of acetobromo-α-D-glucose 2.
Figure 6: a) Schematic diagram for the continuous-flow synthesis of acetobromo-α-D-glucose 2. b) Photograph o...
Scheme 2: Flow Koenigs–Knorr reaction to methyl glycoside 3 with silver triflate.
Scheme 3: Preparation of glycosyl donor 5.
Scheme 4: Two-step glycosylation reactions starting from pyranose 3.
Scheme 5: Synthesis of azide-functionalized glycopyranoside 8.